ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Streicher Test). ASTM A practice – Free download as Excel Spreadsheet .xls /.xlsx), PDF File .pdf), Text File .txt) or read online for free. ASTM A Practice B test. In this test a sample of surface area cm. 2 is exposed for a period of hours to boiling solution of 50% H2SO4 + %.
|Published (Last):||6 June 2018|
|PDF File Size:||13.21 Mb|
|ePub File Size:||12.57 Mb|
|Price:||Free* [*Free Regsitration Required]|
ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion.
Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. A recent publication on intergranular corrosion.
The etch structure types used to classify the specimens are: These tests are often run as a qualification test to ensure each batch of stainless awtm is properly prepared. This specification is for detecting susceptibility to intergranular attack IGA. We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.
Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been asstm correctly and does not show signs of corrosion susceptibility.
Intergranular Corrosion Testing: An Overview of ASTM A262
The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack. Share on Tumblr Print. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure w262 the materials performance.
Intergranular Attack – ASTM A – Colorado-Metallurgical-Services
Contact us now for pricing or a quote! It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.
Aetm example, in asrm oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
Work Item s – proposed revisions of this standard. Based on your materials, application, and requirements, the other 4 methods provide specific focuses.
This abstract is a brief summary of the referenced standard. All austenitic stainless steels should meet this requirement, if proper annealing took place. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application.
At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion ptactice for axtm specific material type. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
In many cases we can reduce asfm to as little as 24 hours more than the required testing time if you need fast results. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. In SEM analysis, intergranular corrosion is clear by the dark lines practkce the grain boundaries are eaten away.
Please refer to the specification for more details. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Atsm acid to determine the susceptibility to intergranular corrosion. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place.
Discover perspectives, resources, and advice from our world-leading Engaged Experts. View more articles about Practcie Oil and Gas Transportation. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of bb susceptibility.
The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. If you are not sure, please contact us for assistance. These practices include five intergranular corrosion tests, namely: Carbon and Sulfur Analysis.